4-Chloro Phenyl Ethyl Amine
₹1,000.00
Applications
4-Chloro Phenyl Ethyl Amine stands as an organic compound belonging to the phenethylamine family. It presents itself as a colorless solid, exhibiting solubility in both water and organic solvents. It finds application in the production of certain insecticides and herbicides.
Description
Description. It is used as a substrate in palladium catalysts on alkaline-earth supports for racemization and dynamic kinetic resolution of benzylic amines. This Thermo Scientific Chemicals brand product was originally part of the Alfa Aesar product portfolio.
Preparation
The invention discloses a method for preparing (4-chlorophenyl)ethylamine, which comprises the following steps: adding a raw material 4-chlorobenzyl cyanide into a hydroborate-chloride reduction system at -15-0 DEG C, and stirring to react in an organic solvent; after the reaction finishes, quenching excessive hydroborate and chloride, carrying out vacuum filtration, reducing the pressure of the filtrate with a water pump, regulating the pH value to 1-5 with dilute acid, extracting with an organic solvent and water, keeping the water phase, regulating the pH value to 8-13 with dilute base, extracting the product with an organic solvent, drying with an anhydrous desiccant, carrying out vacuum filtration, and reducing the pressure of the filtrate with a water pump to remove the filtrate, thereby obtaining the (4-chlorophenyl)ethylamine; and adding an organic solvent, introducing dry hydrogen chloride gas in an ice bath to control the pH value to 1-3, and stirring to obtain (4-chlorophenyl)ethylamine hydrochloride. The method for preparing (4-chlorophenyl)ethylamine has the advantages of higher yield, low cost and no need of column chromatography, and is suitable for large-scale industrial production.
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Description
| Product Name | 4-Chloro Phenyl Ethyl Amine |
| Purity | 98% |
| Molecular Formula | C15H14O3 |
| CAS No | 90-96-0 |
| Molecular Weight | 214 |
| Melting Point | 141 – 143 Deg C |
| Boiling point | 60-65 °C0.1 mm Hg(lit.) |
| Density | 1.112 g/mL at 25 °C(lit.) |
| refractive index | n20/D 1.548(lit.) |
| Flash point | 223 °F |
| storage temp | Store Cold |
| form | Liquid |
| pka | 9.72±0.10(Predicted) |
| Specific Gravity | 1.12 |
| color | Clear colorless to yellow |
4-Chloro Phenyl Ethyl Amine is processed by our vendors using premium quality ingredients. Our offered range is free from any kind of impurity and well known for its accurate composition, long service life and precise pH value. These are highly demanded for their high service and optimum performance.
Our Export Location as a 4-Chloro Phenyl Ethyl Amine Manufacturer, Supplier, Exporter, Stockist from India.
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